Mar 17, 2009 · New PRE-CUT Septa for HPLC Applications. Mar 17 2009. In HPLC often slitted or cross-slitted Silicone/PTFE Septa are used, in order to offer a penetration aid for the fairly thick and dull needles used in the HPLC instruments. While the instrument needle requires the slitted septa, the user may run into the risk of concentration changes due to
Jun 1, 2020 · Quality consistency is one of the basic attributes of medicines, but it is also a difficult problem that natural medicines and their preparations must face. The complex chemical composition and comprehensive pharmacological action of natural medicines make it difficult to simply apply the commonly used evaluation methods in chemical drugs. It is thus urgent to explore the novel evaluation
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Autosampler Vial, 2ml HPLC Vial, Clear Lab Vial, Sample Vial with Writing Area, 9-425 Screw-Thread Vial, Blue Screw Cap with Hole, White PTFE & Red Silicone Septa 100 Pack by Alberts Filter : Amazon.in: Industrial & Scientific
HPLC has many applications in both laboratory and clinical science. It is a common technique used in pharmaceutical development, as it is a dependable way to obtain and ensure product purity. While HPLC can produce extremely high quality (pure) products, it is not always the primary method used in the production of bulk drug materials.
Sep 26, 2016 · The fibrosis assessment results were consistent in 74 out of 80 cases, which accounted for 92.5% of all results gathered. When assessing fibrosis through biopsy, the following percentage distribution was demonstrated: F0 – 26%, F1 – 60%, F2 – 4%, F3 – 4%, and F4 – 6% (Fig. 1).
Purge pump at high flow rate (e.g., 5-10 mL/min.), prime system if necessary. (Prime each pump head separately.) If system has check valve, loosen valve to allow air to escape. If problem persists, flush system with 100% methanol or isopropanol. If problem still persists, contact system manufacturer.
We have been experiencing some pressure problems on our hplc lately and the problem is mostly fluctuations in the pump head.From my little experience i learnt that it may be due to air trapped in
Dec 1, 2016 · A reader’s problem of a method that fails the repeatability requirement of the system suitability test serves as an example of how to approach liquid chromatography (LC) method troubleshooting. I regularly receive questions from readers of “LC Troubleshooting.”. Many of these questions are simple and can be answered with a quick e-mail
PTFE/Silicone septa are the preferred product for use in most HPLC and GC applications where resealability and high purity are critical. PTFE/Silicone septa are offered in a standard formulation as well as a soft durometer formulation recommended for applications where ease of needle penetration is important PTFE/Silicone/PTFE Septa: (T/S/T)
Vial selection for an HPLC system is an important but often overlooked step. Several characteristics of vials and septa are critical for optimum performance in an HPLC run. The following guide will assist you in making the best selection for your specific analysis.
A good SEC-HPLC method is a critical part of the analytical toolbox for biotherapeutics Invest in method development at early stages of the program Critically evaluate the quality of the data SEC-HPLC should be used in conjunction with orthogonal techniques Complementary techniques to give a more complete picture of aggregate
Polyethylene (PE) septa and integral molded closures Chemically resistant polyethylene septa are molded into single-piece caps. The surface for needle penetration is 0.01" thick, allowing for use with most HPLC autosamplers. Polyethylene septa are not resealable and are intended for single injection use with aqueous based sample mixtures.
In the present work, multi-wavelength fusion HPLC nger-printing and UV spectroscopic ngerprinting method were developed for assessing the quality consistency of 35 CLT samples, where the two methods perfectly complement each other. In ngerprint assessments, ALQFM was established for
All HPLC separations are carried out in one of two modes, isocratic or gradient. Isocratic methods separate by using a consistent eluent composition during analysis, like 100% acetonitrile or a 50:50 mixture of acetonitrile to water. On the other hand, gradient methods include a change in the mobile phase composition across a separation.